Structures by: Liang Y. M.
Total: 153
C31H26O
C31H26O
Organic letters (2016) 18, 15 3866-3869
a=11.2411(8)Å b=11.9761(9)Å c=19.9127(14)Å
α=100.200(6)° β=94.644(6)° γ=113.781(7)°
C24H17NO
C24H17NO
Organic letters (2016) 18, 16 4016-4019
a=15.3059(8)Å b=12.1881(6)Å c=9.6280(6)Å
α=90.00° β=90.00° γ=90.00°
C23H30F2N2O2
C23H30F2N2O2
Organic letters (2016) 18, 11 2664-2667
a=13.5393(8)Å b=9.9243(4)Å c=17.0947(10)Å
α=90.00° β=103.566(6)° γ=90.00°
C24H26F2INO4S
C24H26F2INO4S
Organic letters (2015) 17, 17 4280-4283
a=12.1210(6)Å b=15.7186(8)Å c=25.7853(11)Å
α=90.00° β=91.321(4)° γ=90.00°
C23H25F2IN2O4S
C23H25F2IN2O4S
Organic letters (2015) 17, 17 4280-4283
a=24.1416(7)Å b=10.1959(3)Å c=20.5376(6)Å
α=90.00° β=90.00° γ=90.00°
C24H25F3INO4S
C24H25F3INO4S
Organic letters (2015) 17, 17 4280-4283
a=13.4658(3)Å b=20.2837(7)Å c=19.4390(5)Å
α=90.00° β=100.921(2)° γ=90.00°
C28H22O3S
C28H22O3S
Organic Chemistry Frontiers (2019) 6, 17 3162
a=10.465(2)Å b=9.797(2)Å c=22.032(5)Å
α=90° β=95.834(3)° γ=90°
2',3'-dihydrospiro[cyclopentane-1,1'-cyclopenta[a]naphthalen]-2-one
C17H16O
Organic Chemistry Frontiers (2017) 4, 7 1376
a=7.7380(5)Å b=11.6560(8)Å c=14.0895(8)Å
α=90.00° β=90.00° γ=90.00°
C16H11F5O
C16H11F5O
Organic letters (2016) 18, 8 1784-1787
a=22.905(4)Å b=7.8263(9)Å c=15.6010(17)Å
α=90.00° β=90.00° γ=90.00°
C23H17F4NO
C23H17F4NO
Organic letters (2016) 18, 8 1784-1787
a=13.0334(6)Å b=8.6509(4)Å c=17.4221(11)Å
α=90.00° β=101.862(5)° γ=90.00°
C24H19F3O3S,CHCl3
C24H19F3O3S,CHCl3
Organic letters (2016) 18, 7 1514-1517
a=9.3849(5)Å b=19.4808(11)Å c=14.2431(6)Å
α=90.00° β=93.135(4)° γ=90.00°
C26H17F3OS
C26H17F3OS
Organic letters (2016) 18, 7 1514-1517
a=10.9922(6)Å b=34.479(2)Å c=11.1612(5)Å
α=90.00° β=94.851(4)° γ=90.00°
C29H20F5NO2S2
C29H20F5NO2S2
Organic letters (2016) 18, 7 1514-1517
a=19.4188(8)Å b=11.5902(4)Å c=22.8272(6)Å
α=90° β=90° γ=90°
C22H15F3OS
C22H15F3OS
Organic letters (2016) 18, 7 1514-1517
a=13.2577(3)Å b=12.2802(4)Å c=22.5646(5)Å
α=90.00° β=94.431(2)° γ=90.00°
C32H27N2O2P
C32H27N2O2P
Organic letters (2016) 18, 2 216-219
a=14.0310(7)Å b=8.9510(3)Å c=20.9862(11)Å
α=90.00° β=106.794(6)° γ=90.00°
C22H24F3NO3S
C22H24F3NO3S
Organic letters (2016) 18, 14 3486-3489
a=12.2909(8)Å b=12.7985(11)Å c=14.5821(9)Å
α=90.00° β=101.076(6)° γ=90.00°
C32H25N2
C32H25N2
Organic letters (2016) 18, 5 940
a=10.6146(8)Å b=13.7299(11)Å c=16.5455(14)Å
α=90.00° β=90.00° γ=90.00°
C22H20BrF3N2O2S
C22H20BrF3N2O2S
Organic letters (2014) 16, 15 3896-3899
a=12.3141(9)Å b=25.4743(19)Å c=14.8041(9)Å
α=90.00° β=94.832(5)° γ=90.00°
C21H19F3N4O3S
C21H19F3N4O3S
Organic letters (2014) 16, 15 3896-3899
a=16.421(2)Å b=8.6118(12)Å c=16.299(2)Å
α=90° β=104.901(15)° γ=90°
C21H17ClI2O3
C21H17ClI2O3
Organic letters (2014) 16, 8 2236-2239
a=9.6504(11)Å b=10.0633(12)Å c=12.6865(12)Å
α=73.782(10)° β=80.037(9)° γ=62.461(12)°
C21H17I3O3
C21H17I3O3
Organic letters (2014) 16, 8 2236-2239
a=9.5417(5)Å b=10.2550(7)Å c=12.6145(8)Å
α=73.414(6)° β=84.654(5)° γ=68.761(5)°
C14H16F3NO3S
C14H16F3NO3S
Organic letters (2014) 16, 1 270-273
a=5.7301(5)Å b=10.3183(14)Å c=13.7835(17)Å
α=79.233(11)° β=87.668(8)° γ=88.785(9)°
C31H31O5P
C31H31O5P
Organic letters (2014) 16, 21 5616-5619
a=11.5189(13)Å b=20.166(2)Å c=12.1082(10)Å
α=90° β=99.379(10)° γ=90°
C24H23BrN2O7
C24H23BrN2O7
Organic letters (2014) 16, 9 2438-2441
a=9.6196(5)Å b=14.4057(12)Å c=17.108(9)Å
α=90° β=90° γ=90°
C29H24BrNO5
C29H24BrNO5
Organic letters (2014) 16, 6 1802-1805
a=8.9150(5)Å b=11.1839(5)Å c=25.1030(11)Å
α=90° β=90° γ=90°
C28H23NO2S
C28H23NO2S
Organic letters (2012) 14, 13 3344-3347
a=8.568(4)Å b=12.935(6)Å c=20.357(10)Å
α=90.00° β=100.261(5)° γ=90.00°
C22H16IN
C22H16IN
Organic letters (2011) 13, 10 2598-2601
a=5.768(2)Å b=16.473(6)Å c=18.703(7)Å
α=90.00° β=92.573(4)° γ=90.00°
C17H16N2O5
C17H16N2O5
Organic letters (2009) 11, 24 5726-5729
a=9.6975(10)Å b=17.4780(19)Å c=9.6297(10)Å
α=90.00° β=93.354(5)° γ=90.00°
C16H12I2O
C16H12I2O
Organic letters (2011) 13, 4 684-687
a=28.7109(10)Å b=6.0157(2)Å c=20.2899(9)Å
α=90.00° β=120.169(4)° γ=90.00°
C16H10I2
C16H10I2
Organic letters (2012) 14, 8 1990-1993
a=19.513(10)Å b=10.041(5)Å c=16.438(9)Å
α=90.00° β=115.177(4)° γ=90.00°
C21H24O6
C21H24O6
Organic letters (2006) 8, 25 5777-5780
a=11.0511(10)Å b=20.5371(16)Å c=9.0441(8)Å
α=90.00° β=96.047(4)° γ=90.00°
C26H25N
C26H25N
Organic letters (2009) 11, 15 3418-3421
a=10.543(10)Å b=11.806(12)Å c=16.085(15)Å
α=90.00° β=95.60(3)° γ=90.00°
C16H18O2
C16H18O2
Organic letters (2009) 11, 15 3214-3217
a=9.971(11)Å b=8.960(10)Å c=15.880(17)Å
α=90.00° β=103.924(16)° γ=90.00°
C20H17IO4
C20H17IO4
Organic letters (2007) 9, 3 397-400
a=7.615(16)Å b=9.91(2)Å c=12.33(2)Å
α=98.11(2)° β=96.80(2)° γ=96.62(3)°
C21H17NO5
C21H17NO5
Organic letters (2012) 14, 10 2480-2483
a=10.775(13)Å b=21.81(3)Å c=8.143(10)Å
α=90.00° β=108.880(14)° γ=90.00°
C25H19NO3
C25H19NO3
Organic letters (2012) 14, 10 2480-2483
a=12.2143(19)Å b=20.809(3)Å c=7.8088(12)Å
α=90.00° β=101.253(2)° γ=90.00°
C28H23NO2S
C28H23NO2S
Organic letters (2012) 14, 13 3344-3347
a=8.568(4)Å b=12.935(6)Å c=20.357(10)Å
α=90.00° β=100.261(5)° γ=90.00°
C26H24FNO3S
C26H24FNO3S
Organic letters (2012) 14, 13 3344-3347
a=13.030(13)Å b=12.205(12)Å c=15.586(15)Å
α=90.00° β=114.153(11)° γ=90.00°
C22H21ClF3NO2S2
C22H21ClF3NO2S2
Organic letters (2015) 17, 15 3694-3697
a=5.4961(5)Å b=23.7140(19)Å c=17.6522(13)Å
α=90.00° β=96.871(7)° γ=90.00°
C23H27F3O7S
C23H27F3O7S
Organic letters (2015) 17, 15 3694-3697
a=9.578(2)Å b=10.805(3)Å c=12.575(2)Å
α=102.754(18)° β=97.366(15)° γ=93.699(19)°
C20H16INO
C20H16INO
Organic letters (2015) 17, 12 3186-3189
a=7.2355(5)Å b=20.9295(19)Å c=23.0167(15)Å
α=90.00° β=90.00° γ=90.00°
C20H16INO
C20H16INO
Organic letters (2015) 17, 12 3186-3189
a=10.6990(10)Å b=11.7260(11)Å c=22.2683(12)Å
α=94.284(6)° β=101.795(6)° γ=109.369(8)°
C32H25NO4
C32H25NO4
Organic letters (2015) 17, 13 3206-3209
a=6.62144(14)Å b=20.1343(4)Å c=9.3620(2)Å
α=90.00° β=100.915(2)° γ=90.00°
Febuxostat ethanol solvate
C16H16N2O3S,C2H6O
Organic & biomolecular chemistry (2020) 18, 23 4390-4394
a=4.7274(2)Å b=17.7820(5)Å c=10.7340(4)Å
α=90° β=98.994(4)° γ=90°
C14H18BNO2
C14H18BNO2
Organic & biomolecular chemistry (2020) 18, 23 4390-4394
a=10.3720(3)Å b=12.8487(4)Å c=21.0007(8)Å
α=90° β=90° γ=90°
C18H17NO
C18H17NO
Organic & biomolecular chemistry (2018) 16, 42 7792-7796
a=9.6173(10)Å b=12.7178(10)Å c=11.2532(10)Å
α=90.00° β=95.476(10)° γ=90.00°
C18H17NO
C18H17NO
Organic & biomolecular chemistry (2018) 16, 42 7792-7796
a=22.0489(5)Å b=15.0516(3)Å c=18.1612(4)Å
α=90.00° β=108.711(3)° γ=90.00°
C19H19NO
C19H19NO
Organic & biomolecular chemistry (2018) 16, 42 7792-7796
a=9.2569(18)Å b=15.608(2)Å c=10.8924(18)Å
α=90.00° β=105.432(19)° γ=90.00°
C18H16BrNO
C18H16BrNO
Organic & biomolecular chemistry (2018) 16, 42 7792-7796
a=8.4795(3)Å b=11.3762(4)Å c=16.2210(5)Å
α=90.00° β=92.399(3)° γ=90.00°
C39H26
C39H26
Organic & biomolecular chemistry (2011) 9, 21 7461-7467
a=11.398(5)Å b=12.638(5)Å c=20.547(11)Å
α=107.151(12)° β=96.768(12)° γ=103.674(8)°
C26H28O8
C26H28O8
Organic & Biomolecular Chemistry (2008) 6, 6 1040-1045
a=8.5186(6)Å b=14.4133(11)Å c=19.6340(15)Å
α=90.00° β=90.00° γ=90.00°
C26H18INO
C26H18INO
Organic & biomolecular chemistry (2014) 12, 4 643-650
a=9.6284(4)Å b=11.7266(6)Å c=19.1651(9)Å
α=75.073(5)° β=77.631(4)° γ=87.141(4)°
C20H22NO5P
C20H22NO5P
Organic & biomolecular chemistry (2016) 14, 19 4507-4510
a=8.3931(6)Å b=12.0705(7)Å c=19.3724(10)Å
α=90.00° β=95.807(5)° γ=90.00°
C16H16O4
C16H16O4
Organic & biomolecular chemistry (2011) 9, 9 3375-3379
a=13.741(4)Å b=6.0599(16)Å c=17.805(5)Å
α=90.00° β=109.656(3)° γ=90.00°
C30H28Cl2N2
C30H28Cl2N2
Organic & biomolecular chemistry (2011) 9, 14 5028-5033
a=9.4142(9)Å b=16.6090(17)Å c=16.8295(17)Å
α=90.00° β=105.1730(10)° γ=90.00°
C33H28F2N2O4
C33H28F2N2O4
Chemical communications (Cambridge, England) (2020) 56, 84 12729-12732
a=26.9151(4)Å b=13.9396(2)Å c=7.31714(13)Å
α=90° β=90° γ=90°
CHCl3,C23H23FNO2P
CHCl3,C23H23FNO2P
Chemical communications (Cambridge, England) (2020) 56, 34 4704-4707
a=13.7106(3)Å b=10.0817(2)Å c=19.9799(4)Å
α=90° β=91.4380(18)° γ=90°
C19H19ClN2O3
C19H19ClN2O3
Chemical communications (Cambridge, England) (2020) 56, 44 5933-5936
a=9.3251(3)Å b=18.1174(6)Å c=10.1704(4)Å
α=90° β=98.755(3)° γ=90°
2(C20H22N2O2)
2(C20H22N2O2)
Chemical communications (Cambridge, England) (2020) 56, 44 5933-5936
a=18.7868(3)Å b=9.84896(13)Å c=19.3586(3)Å
α=90° β=108.1425(17)° γ=90°
C20H22N2O3
C20H22N2O3
Chemical communications (Cambridge, England) (2020) 56, 44 5933-5936
a=9.4110(5)Å b=9.7287(5)Å c=9.9501(6)Å
α=87.849(4)° β=85.541(5)° γ=72.201(5)°
C17H16FNO2
C17H16FNO2
Chemical communications (Cambridge, England) (2020) 56, 44 5933-5936
a=17.1703(5)Å b=9.1104(2)Å c=19.1959(6)Å
α=90° β=115.406(4)° γ=90°
2(C17H16N2O)
2(C17H16N2O)
Chemical communications (Cambridge, England) (2020) 56, 44 5933-5936
a=11.9106(5)Å b=6.1532(3)Å c=37.0164(17)Å
α=90° β=97.119(4)° γ=90°
C29H23IN2O3S
C29H23IN2O3S
Chemical communications (Cambridge, England) (2020) 56, 9 1421-1424
a=25.670(2)Å b=10.5220(7)Å c=9.8072(12)Å
α=90° β=90° γ=90°
C28H23BrINO3S
C28H23BrINO3S
Chemical communications (Cambridge, England) (2020) 56, 9 1421-1424
a=14.8474(5)Å b=30.0430(15)Å c=26.3798(6)Å
α=90° β=90° γ=90°
C24H22F2N2O3
C24H22F2N2O3
Chemical communications (Cambridge, England) (2016) 52, 68 10396-10399
a=12.2175(2)Å b=15.8782(3)Å c=22.0697(4)Å
α=90.00° β=90.00° γ=90.00°
C28H25ClF4N2O5
C28H25ClF4N2O5
Chemical communications (Cambridge, England) (2016) 52, 68 10396-10399
a=12.8985(11)Å b=14.8772(11)Å c=27.961(3)Å
α=90.00° β=97.992(8)° γ=90.00°
C15H9F5O2
C15H9F5O2
Chemical communications (Cambridge, England) (2018) 54, 18 2256-2259
a=10.7847(11)Å b=8.7041(9)Å c=28.524(4)Å
α=90° β=99.114(10)° γ=90°
C21H19Cl4NO2
C21H19Cl4NO2
Chemical communications (Cambridge, England) (2018) 54, 18 2256-2259
a=12.8660(3)Å b=13.4392(4)Å c=11.7656(4)Å
α=90.00° β=90.00° γ=90.00°
C13H17N5
C13H17N5
Chemical communications (Cambridge, England) (2018) 54, 79 11148-11151
a=20.970(2)Å b=7.2564(6)Å c=17.3888(17)Å
α=90.00° β=106.224(10)° γ=90.00°
C11H13N5
C11H13N5
Chemical communications (Cambridge, England) (2018) 54, 79 11148-11151
a=10.2177(10)Å b=11.0976(11)Å c=19.154(2)Å
α=90.00° β=90.00° γ=90.00°
C13H10N4
C13H10N4
Chemical communications (Cambridge, England) (2018) 54, 79 11148-11151
a=10.7182(8)Å b=7.0388(5)Å c=14.6427(12)Å
α=90.00° β=90.420(7)° γ=90.00°
C11H19N5
C11H19N5
Chemical communications (Cambridge, England) (2018) 54, 79 11148-11151
a=6.8335(13)Å b=9.1979(15)Å c=10.0075(17)Å
α=94.814(14)° β=103.101(15)° γ=96.922(14)°
C13H15N5
C13H15N5
Chemical communications (Cambridge, England) (2018) 54, 79 11148-11151
a=12.0745(8)Å b=9.2802(7)Å c=11.0512(6)Å
α=90.00° β=96.656(5)° γ=90.00°
C30H31F2NO4S
C30H31F2NO4S
Chemical communications (Cambridge, England) (2018) 54, 42 5334-5337
a=13.8373(7)Å b=14.6324(8)Å c=16.7936(8)Å
α=65.506(5)° β=85.068(4)° γ=61.827(5)°
C31H33F2NO5S
C31H33F2NO5S
Chemical communications (Cambridge, England) (2018) 54, 42 5334-5337
a=12.5836(4)Å b=13.0599(5)Å c=17.6689(7)Å
α=90.00° β=91.349(3)° γ=90.00°
Ethyl 2,2-difluoro-2-(2-methoxy-4-(pyrimidin-2-ylamino)phenyl)acetate
C15H15F2N3O3
Chemical communications (Cambridge, England) (2018) 54, 68 9541-9544
a=12.5999(8)Å b=12.8512(7)Å c=13.5479(9)Å
α=63.165(6)° β=62.666(7)° γ=64.519(6)°
7-methyl-1-tosylindoline
C16H17NO2S
Chemical communications (Cambridge, England) (2018) 54, 27 3407-3410
a=15.2125(8)Å b=15.041(2)Å c=12.8713(8)Å
α=90.00° β=90.483(5)° γ=90.00°
(R)-1-((4-bromophenyl)sulfonyl)-2-phenyl-2,3-dihydro-1H-benzo[g]indole
C24H18BrNO2S
Chemical communications (Cambridge, England) (2018) 54, 27 3407-3410
a=11.2737(10)Å b=8.0033(8)Å c=11.9357(10)Å
α=90.00° β=108.605(9)° γ=90.00°
6-nitro-1-tosylindoline
C15H14N2O4S
Chemical communications (Cambridge, England) (2018) 54, 27 3407-3410
a=8.7131(9)Å b=7.8152(8)Å c=21.654(2)Å
α=90.00° β=92.171(9)° γ=90.00°
C28H25N3O2PdS
C28H25N3O2PdS
Chemical communications (Cambridge, England) (2018) 54, 27 3407-3410
a=8.1719(16)Å b=9.5500(11)Å c=15.502(3)Å
α=87.411(13)° β=88.915(16)° γ=80.386(13)°
4-methyl-2-nitro-5-tosyl-5,5a,6,10b-tetrahydroindeno[2,1-b]indole
C23H20N2O4S
Chemical communications (Cambridge, England) (2018) 54, 27 3407-3410
a=12.0329(9)Å b=24.1681(14)Å c=8.5244(5)Å
α=90° β=103.965(7)° γ=90°
C35H35N3O2PdS,C3H7NO
C35H35N3O2PdS,C3H7NO
Chemical communications (Cambridge, England) (2018) 54, 27 3407-3410
a=10.2072(5)Å b=13.9301(10)Å c=15.1016(13)Å
α=66.531(8)° β=75.760(6)° γ=88.492(5)°
C20H16O
C20H16O
Chemical Communications (2019)
a=8.7455(6)Å b=9.5862(9)Å c=9.8123(10)Å
α=63.150(10)° β=73.885(7)° γ=82.681(7)°
C24H24O
C24H24O
Chemical Communications (2019)
a=7.4217(15)Å b=11.0439(17)Å c=12.509(2)Å
α=102.076(15)° β=98.045(16)° γ=106.355(16)°
C24H18O
C24H18O
Chemical Communications (2019)
a=20.5655(10)Å b=6.0870(3)Å c=27.2088(14)Å
α=90.00° β=98.487(5)° γ=90.00°
5-bromo-N-(tert-butyl)-2-(pyridin-2-yl)aniline
C15H17BrN2
Chemical Communications (2019)
a=36.666(4)Å b=16.9718(19)Å c=9.1422(8)Å
α=90° β=90° γ=90°
C16H18N2O
C16H18N2O
Chemical Communications (2019)
a=16.2862(10)Å b=8.9940(5)Å c=18.4405(12)Å
α=90° β=91.429(6)° γ=90°
C35H32N2O2S
C35H32N2O2S
RSC Advances (2014) 4, 17 8914
a=10.1191(6)Å b=9.9999(7)Å c=30.7760(14)Å
α=90° β=96.077(5)° γ=90°
C37H26F2O
C37H26F2O
RSC Advances (2013) 3, 43 19913
a=8.746(14)Å b=9.852(15)Å c=16.48(3)Å
α=104.013(15)° β=99.760(15)° γ=90.639(15)°
C17H15NO
C17H15NO
Chemical communications (Cambridge, England) (2013) 49, 14 1410-1412
a=11.180(9)Å b=7.292(6)Å c=16.780(13)Å
α=90.00° β=100.945(7)° γ=90.00°
C17H17BrO2
C17H17BrO2
Green Chem. (2016) 18, 15 4176
a=9.5598(6)Å b=9.6393(7)Å c=18.0624(12)Å
α=75.207(6)° β=81.884(6)° γ=72.871(6)°
C22H16INO
C22H16INO
Organic & biomolecular chemistry (2014) 12, 4 643-650
a=10.5172(8)Å b=17.5717(6)Å c=20.0963(11)Å
α=90.00° β=90.00° γ=90.00°
C29H28F4N2O5
C29H28F4N2O5
Chemical communications (Cambridge, England) (2016) 52, 68 10396-10399
a=12.4966(6)Å b=9.7777(4)Å c=22.6334(12)Å
α=90.00° β=100.263(4)° γ=90.00°
(S)-1-((4-bromophenyl)sulfonyl)-3-phenyl-2,3-dihydro-1H-benzo[g]indole
C24H18BrNO2S
Chemical communications (Cambridge, England) (2018) 54, 27 3407-3410
a=7.0085(4)Å b=10.9667(7)Å c=26.5254(15)Å
α=90.00° β=90.00° γ=90.00°
C35H32N2O2S
C35H32N2O2S
RSC Advances (2014) 4, 17 8914
a=10.1191(6)Å b=9.9999(7)Å c=30.7760(14)Å
α=90° β=96.077(5)° γ=90°
C20H22O6
C20H22O6
Chemical communications (Cambridge, England) (2009) 34, 36 5451-5453
a=28.20(3)Å b=9.085(9)Å c=17.51(2)Å
α=90.00° β=122.27(3)° γ=90.00°
C15H17ClO2
C15H17ClO2
Organic letters (2009) 11, 15 3214-3217
a=9.4886(18)Å b=8.7358(16)Å c=16.598(3)Å
α=90.00° β=95.417(9)° γ=90.00°
C16H15F3O3S
C16H15F3O3S
Organic letters (2015) 17, 15 3694-3697
a=9.9242(4)Å b=15.9342(6)Å c=10.0614(4)Å
α=90.00° β=106.109(4)° γ=90.00°
C36H26Cl4Fe2N4NiO2
C36H26Cl4Fe2N4NiO2
Acta Crystallographica Section E (2002) 58, 10 m574-m576
a=7.0320(10)Å b=22.455(4)Å c=11.075(2)Å
α=90.00° β=91.36(3)° γ=90.00°
4-{5-(dimethylamino)-2-[(4-(dimethylamino)-2 -iodophenyl)methyl]phenyl}-(3E)-3-Buten-2-one
C21H25IN2O
Acta Crystallographica Section E (2002) 58, 4 o471-o472
a=9.168(3)Å b=10.8840(10)Å c=10.969(2)Å
α=84.830(10)° β=82.21(2)° γ=65.51(2)°